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HRID1742098

反应详情

EQUATION

反应方程式

HRID 1742098 的结构方程式

REACTANTS

反应物

2
结构：CCI
HCID6340

Ethane, iodo-

C2H5I

结构：O=[N+]([O-])c1ccc(Cn2c(-c3ccccc3)n[nH]c2=S)cc1
HCID19010064

未命名化合物

PRODUCTS

生成物

1
结构：CCSc1nnc(-c2ccccc2)n1Cc1ccc([N+](=O)[O-])cc1
HCID10449916

未命名化合物

收率 91%

PROCEDURE

实验过程

Reaction of 2,4-dihydro-4-(4-nitrobenzyl)-5-phenyl-3H-1,2,4-triazole-3-thione with ethyl iodide according to the procedure of Example 6, Part B, gave a 91% yield of the desired product as a solid, mp 107.5°-108.5° C., homogeneous by TLC in 97:3 CH2Cl2 --MeOH; mass spectrum (FAB) m/e 341 (M+1)+.