Azido(trimethyl)stannane → HCID 178441958, compound

Participants

Reaction Steps

Reaction of 3-n-butyl-4-[(2'-cyanobiphenyl-4-yl)methyl]-5-(cyclohexylmethylthio)-4H-1,2,4-triazole (Step A) with trimethyltin azide according to the procedure of Example 18, Step B, gave a 60% yield of the title compound as a white solid, mp 89°-91° C., homogeneous by TLC in 4:1 CH2Cl2 --MeOH; mass spectrum (FAB) m/e 488 (M+1)+.

Provenance & Evidence