Hydrazine hydrate (1:1) → HCID 14745325, compound

HRID 1742460Notes

Reaction equation

HRID 1742460 reaction equation
[NH2:1][CH:2]1[CH2:7][C:6]([CH3:9])([CH3:8])[NH:5][C:4]([CH3:11])([CH3:10])[CH2:3]1.C([CH:14]([CH2:18][CH2:19][CH2:20][C:21](Cl)=[O:22])[C:15](Cl)=[O:16])C.O.[NH2:25][NH2:26]>CO>[CH3:8][C:6]1([CH3:9])[CH2:7][CH:2]([NH:1][C:15](=[O:16])[CH2:14][CH2:18][CH2:19][CH2:20][C:21]([NH:25][NH2:26])=[O:22])[CH2:3][C:4]([CH3:11])([CH3:10])[NH:5]1

Participants

5

Reactant 3

HCID 24654Hydrazine hydrate (1:1)HCID 375244-Amino-2,2,6,6-tetramethylpiperidineHCID 20085793HCID 20085793, compound

Product 1

HCID 14745325HCID 14745325, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

N-(2,2,6,6-tetramethyl-4-piperidinyl)-N'-aminoadipamide was prepared by reacting 4-amino-2,2,6,6-tetramethylpiperidine with ethyl adipoyl chloride, followed by hydrazinolysis of the resulting ester with 85% hydrazine hydrate in methanol.

Sources & evidence

ORD record
ord-25c67a4fbadf438c888b52e04f1fd5f7
Source dataset
uspto-grants-1994_08
Patent number
US05338853

Reaction notes

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