HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 19006687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Nonanoyl chloride | HCID 69819 | — |
| Reactant | HCID 19006674 | HCID 19006674 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19006687 | HCID 19006687 | — |
Reaction Steps
0.1 mol of 2-(4-heptyloxy-2-fluorophenyl)-5-hydroxypyrimidine (prepared from 4-heptyloxy-2-fluorobenzamidine in accordance with Example 1) is dissolved together with 0.12 mol of pyridine in toluene and 0.1 mol of nonanoyl chloride is then added at room temperature. Stirring is then carried out for 12 hours and standard working-up is carried out. 2-(4-Heptyloxy-2-fluorophenyl)-5-nonanoyloxypyrimidine is obtained, C 65 I, Δε=-0.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05340497 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-5c164df9f46c4e7c918288c0d4318c5e |
| Source note | uspto-grants-1994_08 |