HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorobenzaldehyde → 5-(4-(3,4-Dichlorobenzylideneamino)phenyl)thiazolidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorobenzaldehyde | HCID 22710 | — |
| Reactant | 5-(4-Aminophenyl)thiazolidine-2,4-dione | HCID 12850972 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(4-(3,4-Dichlorobenzylideneamino)phenyl)thiazolidine-2,4-dione | HCID 19006058 | 90.1% |
Reaction Steps
Into 20 ml of ethanol were suspended 0.50 g of 5-(4-aminophenyl)-thiazolidine-2,4-dione, and, after added 0.42 g of 3,4-dichlorobenzaldehyde thereto, the suspension was refluxed for 3 hours. After cooling by standing, the crystals deposited were collected by filtration. The crude crystals were recrystallized from ethanol to obtain 0.79 g of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05342850 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-e9a02d51738344c3a0c7633f27cc843d |
| Source note | uspto-grants-1994_08 |