HRID1742827

反应详情

EQUATION

反应方程式

HRID 1742827 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Into 20 ml of ethanol were suspended 0.50 g of 5-(4-aminophenyl)-thiazolidine-2,4-dione, and, after added 0.42 g of 3,4-dichlorobenzaldehyde thereto, the suspension was refluxed for 3 hours. After cooling by standing, the crystals deposited were collected by filtration. The crude crystals were recrystallized from ethanol to obtain 0.79 g of title compound.

WORKUP

后处理

  1. temperaturethe suspension was refluxed for 3 hours
  2. temperatureAfter cooling
  3. filtrationthe crystals deposited were collected by filtration
  4. customThe crude crystals were recrystallized from ethanol