HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloromethylnaphthalene → HCID 22237306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloromethylnaphthalene | HCID 6845 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | N-(3-(Dimethylamino)propyl)methacrylamide | HCID 78882 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 22237306 | HCID 22237306 | — |
Reaction Steps
A 100 ml flask is charged with 1-chloromethyl naphthalene (7.06 g, 40 mmol), DMAPMA (7.48 g, 44 mmol), MEHQ (0.1 g) and acetone (50 ml). The mixture is heated at reflux for 4 hours. The solvent is then removed under vacuum and the resulting gooey DMAPMA.MNQ solidifies upon standing at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07008618B1 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-350849315e6a42c18d12b80387a79d08 |
| Source note | uspto-grants-2006_03 |