反应详情

A 100 ml flask is charged with 1-chloromethyl naphthalene (7.06 g, 40 mmol), DMAPMA (7.48 g, 44 mmol), MEHQ (0.1 g) and acetone (50 ml). The mixture is heated at reflux for 4 hours. The solvent is then removed under vacuum and the resulting gooey DMAPMA.MNQ solidifies upon standing at room temperature.

1. temperatureThe mixture is heated
2. temperatureat reflux for 4 hours
3. customThe solvent is then removed under vacuum
4. customupon standing at room temperature