Benzyl Bromide → HCID 22238298, compound

HRID 1743206Notes

Reaction equation

HRID 1743206 reaction equation
[CH3:1][N:2]([CH3:24])[C:3]1[CH:8]=[CH:7][C:6]([CH:9]2[C:13]3[C:14]([CH3:21])=[C:15]([OH:20])[C:16]([CH3:19])=[C:17]([CH3:18])[C:12]=3[O:11][C:10]2([CH3:23])[CH3:22])=[CH:5][CH:4]=1.[CH2:25](Br)[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[CH2:25]([O:20][C:15]1[C:16]([CH3:19])=[C:17]([CH3:18])[C:12]2[O:11][C:10]([CH3:22])([CH3:23])[CH:9]([C:6]3[CH:7]=[CH:8][C:3]([N:2]([CH3:1])[CH3:24])=[CH:4][CH:5]=3)[C:13]=2[C:14]=1[CH3:21])[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1

Participants

3

Reactant 2

HCID 7498Benzyl BromideHCID 14770387HCID 14770387, compound

Product 1

HCID 22238298HCID 22238298, compoundYield 40%

Procedure

Using 3-[(4-(dimethylamino)phenyl]-2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ol and benzyl bromide, the title compound was obtained in the same manner as in Example 1.

Sources & evidence

ORD record
ord-457e7abb9bfc4a5e8cfc04a5f1a99fef
Source dataset
uspto-grants-2006_03
Patent number
US07008950B1

Reaction notes

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