Benzyl Bromide → HCID 22238276, compound

HRID 1743207Notes

Reaction equation

HRID 1743207 reaction equation
[CH3:1][C:2]1([CH2:15][N:16]2[CH2:21][CH2:20][N:19]([C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[CH2:18][CH2:17]2)[CH2:6][C:5]2[C:7]([CH3:14])=[C:8]([OH:13])[C:9]([CH3:12])=[C:10]([CH3:11])[C:4]=2[O:3]1.[CH2:28](Br)[C:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1>>[CH2:28]([O:13][C:8]1[C:9]([CH3:12])=[C:10]([CH3:11])[C:4]2[O:3][C:2]([CH3:1])([CH2:15][N:16]3[CH2:21][CH2:20][N:19]([C:22]4[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=4)[CH2:18][CH2:17]3)[CH2:6][C:5]=2[C:7]=1[CH3:14])[C:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1

Participants

3

Reactant 2

HCID 7498Benzyl BromideHCID 22238280HCID 22238280, compound

Product 1

HCID 22238276HCID 22238276, compoundYield 48%

Procedure

Using 2,4,6,7-tetramethyl-2-(4-phenyl-1-piperazinyl)methyl-2,3-dihydrobenzofuran-5-ol and benzyl bromide, the title compound was obtained in the same manner as in Example 1.

Sources & evidence

ORD record
ord-7a22e2cc3150461d83e0ce4c46c18b16
Source dataset
uspto-grants-2006_03
Patent number
US07008950B1

Reaction notes

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