Cyanuric chloride → HCID 86597101, compound

Participants

Reaction Steps

100 mg of (3R,6R,7aS)-6-benzyl-6-tert-butoxycarbonylamino-5-oxohexahydropyrrolo[2,1-b]thiazole-3-carboxamide are dissolved in 3 ml of dimethylformamide and reacted with 28.25 mg of cyanuric chloride at room temperature. After 2 hours, the volatile constituents are stripped off in vacuo at 40° C., and the residue is purified on a column (silica gel, mobile phase: diisopropyl ether:methylene chloride=100:10).

Provenance & Evidence