Phenethylamine → HCID 9974211, compound

HRID 1743311Notes

Reaction equation

HRID 1743311 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]2[C:14]([C:15]=1Cl)=[CH:13][CH:12]=[CH:11][C:10]=2[N+:17]([O-])=O)=[O:5])[CH3:2].[CH2:20]([NH2:28])[CH2:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]2[C:14]([C:15]=1[NH:28][CH2:20][CH2:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)=[CH:13][CH:12]=[CH:11][C:10]=2[NH2:17])=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 1001PhenethylamineHCID 11196760Ethyl 4-chloro-8-nitroquinoline-3-carboxylate

Product 1

HCID 9974211HCID 9974211, compoundYield 88%

Procedure

The compound prepared in Example 3 was reacted with phenethylamine according to the method as described in Example 4 and the obtained compound was treated as described in Example 14 to prepare the title compound (yield 88%).

Workup

  1. additionthe obtained compound was treated

Sources & evidence

ORD record
ord-faefd2a78af5485aa3a08790109298e9
Source dataset
uspto-grants-2006_03
Patent number
US07009053B2

Reaction notes

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