HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 2766903, compound → HCID 12009927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 2766903 | HCID 2766903 | — |
| Reactant | Sodium Hypochlorite | HCID 23665760 | — |
| Product | HCID 12009927 | HCID 12009927 | — |
Reaction Steps
The oxidation of 5-bromo-2-allyloxybenzaldoxime using sodium hypochlorite solution to give 5-bromo-2-allyloxybenzonitrile oxide and the subsequent 1,3-dipolar cycloaddition were carried out in a static micromixer (Technical University of Ilmenau, Faculty of Machine Construction, Dr. Norbert Schwesinger, Postfach 100565, D-98684 Ilmenau) having a physical size of 40 mm×25 mm×1 mm with a total of 11 mixing stages each with a volume of 0.125 μl. The total pressure loss was about 1000 Pa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07009059B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-a756163fb8ef4510bc750c0233f18722 |
| Source note | uspto-grants-2006_03 |