HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 22235510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-[2-(Oxiran-2-yl)ethoxy]benzonitrile | HCID 22235395 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 22235510 | HCID 22235510 | 93% |
Reaction Steps
4-[2-(2-Oxiranyl)ethoxy]benzonitrile (38.5 g, 204 mmol; from step (d) above) was mixed with NH3 (1200 mL, conc.) and isopropanol (450 mL). The mixture was stirred at r.t for 24 h. The solid (by-product) was filtered off and the solvents were evaporated, to give 39.1 g (93%) of sub-title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07012074B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-d82a0e66b3e94ca48634b78a404a60f1 |
| Source note | uspto-grants-2006_03 |