Nitroethane → HCID 69661384, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of the product from Step D (0.64 g, 2.95 mmol) and ammonium acetate (0.23 g, 2.98 mmol) in nitroethane (3 ml) was heated at 115° C. for 2.5 h. The mixture was cooled and the orange solid that formed was collected by filtration, washed with EtOAc and water and dried under vacuum (0.54 g, 67%): mp 240-242° C.

Provenance & Evidence