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HRID1744536

反应详情

EQUATION

反应方程式

HRID 1744536 的结构方程式

REACTANTS

反应物

3
结构：CNCCO
HCID8016

N-Methyl-N-hydroxyethylamine

C3H9NO

结构：CN(CCO)C1CCN(c2ccc([N+](=O)[O-])cc2C#N)CC1
HCID17822771

未命名化合物

结构：N#Cc1cc([N+](=O)[O-])ccc1N1CCC(=O)CC1
HCID22227987

未命名化合物

PRODUCTS

生成物

1
结构：CN(CCO)C1CCN(c2ccc(N)cc2C#N)CC1
HCID22228081

未命名化合物

PROCEDURE

实验过程

According to Tetrahedron, vol. 38, No. 3, p. 413 (1982) and using 5-nitro-2-(4-oxopiperidino) benzonitrile and N-methylethanolamine, 2-[4-(N-2-hydroxyethyl-N-methylamino) piperidin-1-yl]-5-nitrobenzonitrile was synthesized, which was subjected to reduction according to Starting Material Synthesis Example 40 to give the title compound.

WORKUP

后处理

  1. customwas synthesized
  2. customaccording to Starting Material Synthesis Example 40