HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → 7-Butoxy-1,8-difluorofluoren-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 7-Butoxy-1,8-difluorofluorene-2-boronic acid | HCID 22223115 | — |
| Solvent | tert-Butyl methyl ether | HCID 15413 | — |
| Product | 7-Butoxy-1,8-difluorofluoren-2-ol | HCID 22223127 | — |
Reaction Steps
The oxidation of 24 mmol of 7-butoxy-1,8-difluorofluorene-2-boronic acid with 22 ml of hydrogen peroxide (35 percent) in 60 ml of tert-butyl methyl ether is effected in a similar manner to the procedure described in Example 1. 7-Butoxy-1,8-difluorofluoren-2-ol is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018685B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-fbe8386bd9414077907828e30b547124 |
| Source note | uspto-grants-2006_03 |