Ethanol → HCID 90791087, compound

HRID 1744773Notes

Reaction equation

HRID 1744773 reaction equation
[C@@H:1]12[CH2:7][C:6](=[CH:8][C:9]([OH:11])=[O:10])[C@@H:5]1[CH2:4][CH:3]=[CH:2]2.S(=O)(=O)(O)O.[CH2:17](O)[CH3:18]>>[C@@H:1]12[CH2:7][C:6](=[CH:8][C:9]([O:11][CH2:17][CH3:18])=[O:10])[C@@H:5]1[CH2:4][CH:3]=[CH:2]2

Participants

4

Reactant 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 69590722HCID 69590722, compound

Product 1

HCID 90791087HCID 90791087, compound

Conditions

Temperature
80 °C

Procedure

The compound of Example 2 was dissolved in ethanol (20 ml) and concentrated sulfuric acid was added. The reaction was heated to 80° C. and stirred for 18 hours. The solvent was removed in vacuo to yield the title compound as an oil.

Workup

  1. customThe solvent was removed in vacuo

Sources & evidence

ORD record
ord-8e26f581384649719d41db943ce745d0
Source dataset
uspto-grants-2006_03
Patent number
US07018818B2

Reaction notes

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