Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 69590722 | HCID 69590722 | — |
| Product | HCID 90791087 | HCID 90791087 | — |
Reaction Steps
The compound of Example 2 was dissolved in ethanol (20 ml) and concentrated sulfuric acid was added. The reaction was heated to 80° C. and stirred for 18 hours. The solvent was removed in vacuo to yield the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07018818B2 |
|---|
| Source dataset | uspto-grants-2006_03 |
|---|
| ORD ID | ord-8e26f581384649719d41db943ce745d0 |
|---|
| Source note | uspto-grants-2006_03 |
|---|
