Ethylparaben → HCID 22225393, compound

Participants

Reaction Steps

Ethyl 4-hydroxybenzoate (0.128 mmol) was suspended in THF (1 ml) and NaH (2.9 mg, 0.12 mmol) was added. After formation of the subsequent sodium salt, suspended in THF, the resin (A3) was added and shaking continued for 18 h. The resin was washed with THF (2×1 min), DMF (3×1 min, 60° C.) and with DCM (3×1 min).

Provenance & Evidence