huagongshe.com
HRID1744817

反应详情

EQUATION

反应方程式

HRID 1744817 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)C1(Cc2ccccc2)CCN(Cc2ccccc2)CC1
HCID10497176

1,4-dibenzyl-piperidine-4-carboxylic acid ethyl ester

C22H27NO2

结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

PRODUCTS

生成物

1
结构：OCC1(Cc2ccccc2)CCN(Cc2ccccc2)CC1
HCID22225015

未命名化合物

收率 81%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Was prepared from 1,4-dibenzyl-piperidine-4-carboxylic acid ethyl ester (J. Chem. Soc., Perkin Trans. 1 1996, 20, 2545–2551.) by lithium aluminium hydride reduction in tetrahydrofurane under standard conditions in 81% yield. MS 296(M+H+).