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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1744954Generated: November 3, 2026

HCID 11172083, compound → HCID 11229736, compound

https://huagongshe.com/reaction/1744954

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 11172083HCID 11172083—
SolventManganese dioxideHCID 14801—
Solventdichloromethane N,N-dimethylformamideHCID 22350042—
ProductHCID 11229736HCID 11229736—

Reaction Steps

2-Formyl-7-fluoro-imidazo[2,1-b]-benzthiazole was prepared according to the procedure outlined in Example 1, (Step 3). Starting from 7-fluoro-imidazo[2,1-b]-benzthiazole-2-methanol (1.5 g 6.7 mmol) in methylene chloride/DMF(300 mL: 50 mL) and active MnO2 (12 g, excess), 1.1 g (78% Yield) of the aldehyde derivative was isolated as brown solid. (M+H) 221.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07018997B2
Source datasetuspto-grants-2006_03
ORD IDord-7b1f9987bf404ed99f2a8e4ed70ad456
Source noteuspto-grants-2006_03