2-Methoxyethylamine → HCID 131725524, compound

HRID 1745178Notes

Reaction equation

[CH2:1]([O:4][N:5]=[C:6]1[CH2:10][N:9](C(OC(C)(C)C)=O)[C@H:8]([C:18]([OH:20])=O)[CH2:7]1)[CH:2]=[CH2:3].[CH3:21][O:22][CH2:23][CH2:24][NH2:25]>>[CH2:1]([O:4][N:5]=[C:6]1[CH2:10][NH:9][C@H:8]([C:18]([NH:25][CH2:24][CH2:23][O:22][CH3:21])=[O:20])[CH2:7]1)[CH:2]=[CH2:3]

Participants

Reactant 2

HCID 80182-Methoxyethylamine

HCID 58714562(2S,4EZ)-4-[(allyloxy)imino)-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acid

Product 1

HCID 131725524HCID 131725524, compound

Procedure

Following the general method as outlined in Example 22, starting from (2S,4EZ)-4-[(allyloxy)-imino]-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acid, and 2-methoxyethylamine the title compound was obtained in 100% purity by LC/MS. MS(ESI+): m/z=242.0.

Sources & evidence

ORD record: ord-d569fb62823f4e43b0adfbe845b3971d
Source dataset: uspto-grants-2006_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07018988B2

Reaction notes

Loading…