HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo-1,3-dioxole-5-methylamine → HCID 69250312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo-1,3-dioxole-5-methylamine | HCID 75799 | — |
| Reactant | 4-Phenylbenzoyl chloride | HCID 84151 | — |
| Reactant | HCID 69251379 | HCID 69251379 | — |
| Product | HCID 69250312 | HCID 69250312 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(chloromethylene)-2-pyrrolidinecarboxylic acid, [1,1′-biphenyl]-4-carbo-nyl chloride, and 1,3-benzodioxol-5-ylmethylamine the title compound was obtained in 63% purity by LC/MS. MS(ESI+): m/z=475.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018988B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-5f1406d67cbf4fa484b55f6a7185e685 |
| Source note | uspto-grants-2006_03 |