HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenemethanamine → HCID 131725567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenemethanamine | HCID 8355 | — |
| Reactant | 4-(Dimethylamino)butanoyl chloride | HCID 15087690 | — |
| Reactant | (2S,4EZ)-4-[(allyloxy)imino)-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acid | HCID 58714562 | — |
| Product | HCID 131725567 | HCID 131725567 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from (2S,4EZ)-4-[(allyloxy)imino]-1-(tert-butoxycarbonyl)-2-pyrrolidinecarboxylic acid, 4-(dimethylamino)buta-noyl chloride, and 1-naphthylmethylamine the title compound was obtained in 85% purity by LC/MS. MS(ESI+): m/z=437.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018988B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-f684da39a5ea4c83bdde4b6f02dfd766 |
| Source note | uspto-grants-2006_03 |