HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54189546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Chlorothiophene-2-carbonyl chloride | HCID 2735824 | — |
| Reactant | Potassium ethyl malonate | HCID 3446434 | — |
| Reactant | Magnesium Chloride | HCID 5360315 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54189546 | HCID 54189546 | — |
Reaction Steps
Prepared from 3-chloro-2-thiophenecarbonyl chloride [CAS-No. 86427-02-3] by reaction with ethyl malonate potassium salt with Et3N and MgCl2 in CH3CN according to general procedure H (method a). Obtained as a brown oil (6.84 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07018998B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-d559bbe00a664b9c870cdee7218b74c5 |
| Source note | uspto-grants-2006_03 |