HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → HCID 86655463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | (S)-Methyl 2-amino-3-(4-methoxyphenyl)propanoate hydrochloride | HCID 69612215 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86655463 | HCID 86655463 | 58% |
Reaction Steps
The same procedures as in Example 1 were carried out from the compound obtained in Example 33 (3.3 g), acrylic acid (1.1 mL), DCC (3.4 g), triethylamine (9.5 mL, 68.2 mmol), and chloroform (140 mL), to give the captioned compound (2.1 g, 58%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-1f855bd5f4df4e9ab1b2290a6160ee70 |
| Source note | uspto-grants-2015_10 |