HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67311344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(2-Fluorophenyl)prop-2-enoic acid | HCID 67977 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | L-Methionine, methyl ester, hydrochloride | HCID 11435579 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67311344 | HCID 67311344 | 95% |
Reaction Steps
The same procedures as in Example 2 were carried out from methyl L-methioninate hydrochloride (2.5 g), triethylamine (2.1 mL), 2-fluorocinnamic acid (2.5 g), WSC.HCl (2.9 g, 15.0 mmol), and methylene chloride (80 mL), to give the captioned compound (3.7 g, 95%) as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-45f39a3c6da44bdface52d299ff45384 |
| Source note | uspto-grants-2015_10 |