HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 67130504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 86655521 | HCID 86655521 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67130504 | HCID 67130504 | 92% |
Reaction Steps
The same procedures as in Example 29 were carried out from the compound obtained in Example 113 (3.8 g), 4 mol/L of hydrogen chloride-dioxane (7.0 mL), and methylene chloride (80 mL), to give the captioned compound (3.0 g, 92%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-67c8fe6f8c04434e8b4dcac635544676 |
| Source note | uspto-grants-2015_10 |