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HRID1746584

反应详情

EQUATION

反应方程式

HRID 1746584 的结构方程式

REACTANTS

反应物

3
结构：O=C1CCC(=O)N1O
HCID80170

2,5-Pyrrolidinedione, 1-hydroxy-

C4H5NO3

结构：N#Cc1ccc(C=CC(=O)O)cc1
HCID86773

3-(4-Cyanophenyl)-2-propenoic acid

C10H7NO2

结构：CCN=C=NCCCN(C)C.Cl
HCID2723939

1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride

C8H18ClN3

PRODUCTS

生成物

1
结构：N#Cc1ccc(C=CC(=O)ON2C(=O)CCC2=O)cc1
HCID86655525

未命名化合物

收率 79.5%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The same procedures as in Example 117 were carried out from 4-cyanocinnamic acid (5.0 g), N-hydroxysuccinic acid imide (5.0 g), WSC.HCl (8.3 g), and methylene chloride (150 mL), to give the captioned compound (6.2 g, 79%) as crystals.