HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 67130572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 67130680 | HCID 67130680 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67130572 | HCID 67130572 | 63% |
Reaction Steps
The same procedures as in Example 143 were carried out from the compound obtained in Example 142 (4.2 g), 4 mol/L of hydrogen chloride-dioxane solution (14.0 mL), and methylene chloride (140 mL), to give the captioned compound (2.2 g, 63%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-e59708f322d846f18fe9e1820cf7413c |
| Source note | uspto-grants-2015_10 |