HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67130477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(2-Fluorophenyl)prop-2-enoic acid | HCID 67977 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | HCID 67130445 | HCID 67130445 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67130477 | HCID 67130477 | 98% |
Reaction Steps
The same procedures as in Example 146 were carried out from the compound obtained in Example 144 (0.7 g), triethylamine (0.4 mL), 2-fluorocinnamic acid (0.44 g), WSC.HCl (0.50 g), and methylene chloride (20 mL), to give the captioned compound (0.9 g, 98%) as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-3e0aba70b08043f082e253356c00cc1b |
| Source note | uspto-grants-2015_10 |