HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67311725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(2-Fluorophenyl)prop-2-enoic acid | HCID 67977 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | HCID 67130572 | HCID 67130572 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67311725 | HCID 67311725 | 77.2% |
Reaction Steps
The same procedures as in Example 146 were carried out from the compound obtained in Example 145 (2.0 g), triethylamine (1.0 mL), 2-fluorocinnamic acid (1.2 g), WSC.HCl (1.4 g), and methylene chloride (60 mL), to give the captioned compound (2.1 g, 77%) as an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-46636c7d402c4480baa087645d87656d |
| Source note | uspto-grants-2015_10 |