HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 67130661, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 67130653 | HCID 67130653 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67130661 | HCID 67130661 | 81% |
Reaction Steps
The same procedures as in Example 143 were carried out from the compound obtained in Example 152 (12.2 g), 4 mol/L of hydrogen chloride-dioxane solution (31 mL), and methylene chloride (300 mL), to give the captioned compound (8.6 g, 81%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150510B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-17a1adef001449c0a138837312b4a487 |
| Source note | uspto-grants-2015_10 |