HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1,3-diiodo- → HCID 89560253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1,3-diiodo- | HCID 12270 | — |
| Reactant | (3aS)-Tetrahydro-1H,3H-1lambda~6~-pyrrolo[1,2-c][1,2,3]oxathiazole-1,1-dione | HCID 23255919 | — |
| Product | HCID 89560253 | HCID 89560253 | — |
Reaction Steps
(S)-2-(3-Iodo-benzyl)-pyrrolidine was prepared from 1,3-diiodobenzene and (S)-tetrahydro-pyrrolo[1,2-c][1,2,3]oxathiazole 1,1-dioxide in analogy to the procedure described for Example 4 in U.S. Pat. No. 5,130,432. LC-MS A: tR=0.57 min; [M+H]+=287.99.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150566B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-fe884003f5d54b3e87788e7bb2c69122 |
| Source note | uspto-grants-2015_10 |