HRID1747374

反应详情

EQUATION

反应方程式

HRID 1747374 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of (S)-3-(2-Nitro-phenylamino)-hexanoic acid ethyl ester (795 mg, 2.8 mmol) in EtOH (20 mL) was added Pd/C (10% wt on carbon) (300 mg). The solution was stirred at room temperature for 3 hours. The solution was filtered and the filtrate was concentrated. The residue (683 mg, 96%) was used in the next step of the synthesis without further purification.

WORKUP

后处理

  1. filtrationThe solution was filtered
  2. concentrationthe filtrate was concentrated
  3. customThe residue (683 mg, 96%) was used in the next step of the synthesis without further purification