HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59497561, compound → HCID 59497419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59497561 | HCID 59497561 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59497419 | HCID 59497419 | 91.3% |
Reaction Steps
3-(2-Ethoxycarbonyl-ethylamino)-4-nitro-benzoic acid tert-butyl ester (1.2 g, 3.55 mmol) was dissolved in ethanol (60 ml) to the solution Pd/C (10%) (300 mg) was added and the reaction mixture was stirred under Hydrogen (1 atmosphere) overnight. The reaction mixture was filtered through celite and evaporated to dryness to give 1 g (91%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150556B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-48e1335345014e0bb8476d01ed21dd04 |
| Source note | uspto-grants-2015_10 |