HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71293991, compound → HCID 71294061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71293991 | HCID 71293991 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 71294061 | HCID 71294061 | 102.9% |
Reaction Steps
Compound B3 (48.9 mg, 0.0880 mmol) obtained in Step 1 was dissolved in trifluoroacetic acid (1.0 mL) and the solution was stirred at room temperature for 20 minutes. The solvent was evaporated under reduced pressure. The residue was purified by silica gel column chromatography (hexane/ethyl acetate=1/1) to give Compound 42 (38.6 mg, 100% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150569B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-cb89e57f586b423ba9330f165280cc4e |
| Source note | uspto-grants-2015_10 |