Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1747557Generated: November 1, 2026

HCID 71293991, compound → HCID 71294061, compound

https://huagongshe.com/reaction/1747557

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 71293991HCID 71293991—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 71294061HCID 71294061102.9%

Reaction Steps

Compound B3 (48.9 mg, 0.0880 mmol) obtained in Step 1 was dissolved in trifluoroacetic acid (1.0 mL) and the solution was stirred at room temperature for 20 minutes. The solvent was evaporated under reduced pressure. The residue was purified by silica gel column chromatography (hexane/ethyl acetate=1/1) to give Compound 42 (38.6 mg, 100% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09150569B2
Source datasetuspto-grants-2015_10
ORD IDord-cb89e57f586b423ba9330f165280cc4e
Source noteuspto-grants-2015_10