HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 86723592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 58072472 | HCID 58072472 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86723592 | HCID 86723592 | — |
Reaction Steps
5-Methoxy-3-(1-phenyl-1H-pyrazol-5-yl)-1-pyridin-4-ylpyridazin-4(1H)-one (0.49 g) and benzylbromide (0.25 mL) were dissolved in acetonitrile (30 mL), and the mixture was heated under reflux overnight. The solvent was evaporated under reduced pressure, and the obtained crystals were washed with ethyl acetate to give the title compound (0.73 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150588B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-ed27ad0946f94b328c5d560d8fd02e73 |
| Source note | uspto-grants-2015_10 |