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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1748422Generated: November 1, 2026

2-Aminothiophenol → HCID 136483032, compound

https://huagongshe.com/reaction/1748422

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-AminothiophenolHCID 8713—
Reactant3,5-Di-tert-butylsalicylaldehydeHCID 688023—
SolventBenzeneHCID 241—
ProductHCID 136483032HCID 136483032—

Reaction Conditions

Temperature100 °C

Reaction Steps

A solution of 3,5-di-tert-butyl-2-hydroxybenzaldehyde (6.79 g, 0.03 mol) in benzene (50 mL) was added to a solution of 2-Aminothiophenol (3.63 g, 0.03 mol) in benzene (50 mL) and heated at 100° C. in closed glass vessel for 3 days. The solvent was removed in vacuum. The product was obtained as a yellow oil in a quantitative yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09150676B2
Source datasetuspto-grants-2015_10
ORD IDord-2a3b5f9d65c14c5997cebff1c5831674
Source noteuspto-grants-2015_10