HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 16794101, compound → HCID 86692527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 16794101 | HCID 16794101 | — |
| Reactant | HCID 86692528 | HCID 86692528 | — |
| Product | HCID 86692527 | HCID 86692527 | — |
Reaction Steps
4-[4-(5-Bromo-3-fluoropyridin-2-yl)cyclohex-3-en-1-yl]morpholine (2.28 g) was used in place of 1-(5-bromopyridin-2-yl)-c-4-(tert-butyldimethyl silanyloxy)-r-1-cyclohexanecarbonitrile in Reference Example 144 (2) and (3), and reacted and treated in a similar manner to give the titled compound (1.68 g) as a pale yellow solid. MS (ESI) m/z: 278 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150555B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-f82bea6294644355b99734bf36fd2b91 |
| Source note | uspto-grants-2015_10 |