HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 16794101, compound → HCID 178455310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 16794101 | HCID 16794101 | — |
| Reactant | HCID 178455308 | HCID 178455308 | — |
| Product | HCID 178455310 | HCID 178455310 | — |
Reaction Steps
trans-5-Bromo-2-[4-(tert-butyldimethylsilyloxy)cyclohex-1-yl]pyridine (1.54 g) described in Reference Example 103 (3) was used in place of 1-(5-bromopyridin-2-yl)-c-4-(tert-butyldimethylsilanyloxy)-r-1-cyclohexanecarbonitrile in Reference Example 144 (2) and (3), and reacted and treated in a similar manner to give the titled compound (1.11 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150555B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-5c0118ecbb4f4808b495d0f3aad4f9d8 |
| Source note | uspto-grants-2015_10 |