HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 16794101, compound → HCID 86692533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 16794101 | HCID 16794101 | — |
| Reactant | HCID 57803252 | HCID 57803252 | — |
| Product | HCID 86692533 | HCID 86692533 | — |
Reaction Steps
8-(5-Bromopyridin-2-yl)-1,4-dioxaspiro[4.5]decan-8-ol (3.0 g) described in Reference Example 76 (1) was used in place of 1-(5-bromopyridin-2-yl)-c-4-(tert-butyldimethylsilanyloxy)-r-1-cyclohexanecarbonitrile in Reference Example 144 (2) and (3), and reacted and treated in a similar manner to give the titled compound (1.28 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150555B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-dbcb282dea4045029335808c6acbe28e |
| Source note | uspto-grants-2015_10 |