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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1748741Generated: October 30, 2026

Thioglycolic Acid → HCID 136348426, compound

https://huagongshe.com/reaction/1748741

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThioglycolic AcidHCID 1133—
Reactant2,4-DichlorobenzaldehydeHCID 13404—
ReactantHCID 86724082HCID 86724082—
ProductHCID 136348426HCID 136348426—

Reaction Steps

tert-Butyl(2S)-2-[4-(2,4-dichlorophenyl)-1-methyl-4,6,7,8-tetrahydropyrazolo[3,4-e][1,4]thiazepin-3-yl]pyrrolidine-1-carboxylate was prepared according to procedure C using tert-butyl (2S)-2-(5-amino-1-methyl-pyrazol-3-yl)pyrrolidine-1-carboxylate, thioglycolic acid and 2,4-dichlorobenzaldehyde. The resulting amide was reduced according to procedure D and the material was used directly in Step D below.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09150592B2
Source datasetuspto-grants-2015_10
ORD IDord-d67964cd9a2c47ffb86f948353e6099b
Source noteuspto-grants-2015_10