HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioglycolic Acid → HCID 136348426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | 2,4-Dichlorobenzaldehyde | HCID 13404 | — |
| Reactant | HCID 86724082 | HCID 86724082 | — |
| Product | HCID 136348426 | HCID 136348426 | — |
Reaction Steps
tert-Butyl(2S)-2-[4-(2,4-dichlorophenyl)-1-methyl-4,6,7,8-tetrahydropyrazolo[3,4-e][1,4]thiazepin-3-yl]pyrrolidine-1-carboxylate was prepared according to procedure C using tert-butyl (2S)-2-(5-amino-1-methyl-pyrazol-3-yl)pyrrolidine-1-carboxylate, thioglycolic acid and 2,4-dichlorobenzaldehyde. The resulting amide was reduced according to procedure D and the material was used directly in Step D below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150592B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-d67964cd9a2c47ffb86f948353e6099b |
| Source note | uspto-grants-2015_10 |