HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-L-Valine → HCID 131733567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-L-Valine | HCID 83693 | — |
| Reactant | N~2~,N~6~-Bis{[(9H-fluoren-9-yl)methoxy]carbonyl}-L-lysine | HCID 13783708 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131733567 | HCID 131733567 | — |
Reaction Steps
Dry Versabeads A-1900 (315-500 μm, 0.2 mmol NH2/g) (1.20 g) were dissolved in dry DMF (10 mL) and coupled with FmocLys(Fmoc)OH (0.24 mmol, 1 eq) and Boc-ValOH (0.48 mmol, 2 eq) using the general SPPS coupling procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09150899B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-dc7416805feb49c49a6c33eb89491d51 |
| Source note | uspto-grants-2015_10 |