化工社化工社 化学情報印刷レポート · 研究参考用
Cadmium Nitrate → Tetradecanoic acid, cadmium salt (2:1)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cadmium Nitrate | HCID 25154 | — |
| 反応物 | Sodium Myristate | HCID 23693095 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Tetradecanoic acid, cadmium salt (2:1) | HCID 66290 | — |
反応手順
A solution of cadmium nitrate in methanol was added to a solution of sodium myristate, also in methanol. To obtain high quality cadmium myristate, the sodium myristate solution was heated to about 90° C. until all of the particles are dissolved. Afterward, the cadmium nitrate solution was injected slowly, drop-wise, and the reaction was allowed to take place. The temperature was then reduced to room temperature where the cadmium myristate powder began to precipitate below 65° C. The powder was then collected, filtered, and dried in a box oven. The dried cake was then crushed to produce fine particles of cadmium myristate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09151668B1 |
| 出典データセット | uspto-grants-2015_10 |
| ORD ID | ord-9ece35995482423c8ecc348f9e5f9a29 |
| 出典メモ | uspto-grants-2015_10 |