2-Aminothiophenol → HCID 4659104, compound

HRID 1748971Notes

Reaction equation

HRID 1748971 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[SH:8].[Br:9][C:10]1[CH:11]=[C:12]([CH:15]=[C:16]([Br:19])[C:17]=1[OH:18])[CH:13]=O>CO>[S:8]1[C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[N:1]=[C:13]1[C:12]1[CH:11]=[C:10]([Br:9])[C:17]([OH:18])=[C:16]([Br:19])[CH:15]=1

Participants

4

Reactant 2

HCID 87132-AminothiophenolHCID 181003,5-Dibromo-4-Hydroxybenzaldehyde

Product 1

HCID 4659104HCID 4659104, compoundYield 16%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a methanol solvent, a solution including 2-aminothiophenol (1.0 eq.) and 3,5-dibromo-4-hydroxybenzaldehyde (1.0 eq.) was stirred at room temperature. The produced precipitate was filtered and the filtered product was washed with cold methanol to obtain Compound 27.

Workup

  1. filtrationThe produced precipitate was filtered
  2. washthe filtered product was washed with cold methanol

Sources & evidence

ORD record
ord-cb97f3c3d7174d029e0fcfe51175bb04
Source dataset
uspto-grants-2015_10
Patent number
US09155690B2

Reaction notes

Loading…