HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminothiophenol → HCID 4659104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminothiophenol | HCID 8713 | — |
| Reactant | 3,5-Dibromo-4-Hydroxybenzaldehyde | HCID 18100 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 4659104 | HCID 4659104 | 16% |
Reaction Steps
In a methanol solvent, a solution including 2-aminothiophenol (1.0 eq.) and 3,5-dibromo-4-hydroxybenzaldehyde (1.0 eq.) was stirred at room temperature. The produced precipitate was filtered and the filtered product was washed with cold methanol to obtain Compound 27.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09155690B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-cb97f3c3d7174d029e0fcfe51175bb04 |
| Source note | uspto-grants-2015_10 |