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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1749549Generated: October 29, 2026

HCID 131733594, compound → HCID 118162113, compound

https://huagongshe.com/reaction/1749549

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 131733594HCID 131733594—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 118162113HCID 118162113120.6%

Reaction Conditions

Temperature25 °C

Reaction Steps

A mixture of benzyl ((1R,3S)-3-carbamoyl-2,2-dimethylcyclobutyl)carbamate (193 mg, 0.70 mmol) and palladium on activated carbon (10% Pd, 30 mg) in MeOH (5 mL) was stirred at 25° C. under hydrogen atmosphere for 5 h. The reaction mixture was filtered through celite and the filtrate was concentrated to afford the crude title compound (120 mg, crude). MS (ESI) m/z 143.1 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09156798B2
Source datasetuspto-grants-2015_10
ORD IDord-2360b4730ab048eba0315a789e9d5b45
Source noteuspto-grants-2015_10