HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1749549Generated: October 29, 2026
HCID 131733594, compound → HCID 118162113, compound
https://huagongshe.com/reaction/1749549
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 131733594 | HCID 131733594 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 118162113 | HCID 118162113 | 120.6% |
Reaction Steps
A mixture of benzyl ((1R,3S)-3-carbamoyl-2,2-dimethylcyclobutyl)carbamate (193 mg, 0.70 mmol) and palladium on activated carbon (10% Pd, 30 mg) in MeOH (5 mL) was stirred at 25° C. under hydrogen atmosphere for 5 h. The reaction mixture was filtered through celite and the filtrate was concentrated to afford the crude title compound (120 mg, crude). MS (ESI) m/z 143.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09156798B2 |
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| Source dataset | uspto-grants-2015_10 |
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| ORD ID | ord-2360b4730ab048eba0315a789e9d5b45 |
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| Source note | uspto-grants-2015_10 |
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