HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178488169, compound → HCID 178488168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178488169 | HCID 178488169 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178488168 | HCID 178488168 | 70% |
Reaction Steps
A solution of (5-methoxy-1H-indazol-3-yl)methanol (0.367 g, 2.06 mmol) in ethyl acetate (20 mL) was added with manganese dioxide (1.79 g, 20.6 mmol), and the mixture was stirred overnight at room temperature. The reaction mixture was filtered through Celite, and then the filtrate was concentrated to obtain 5-methoxy-1H-indazole-3-carbaldehyde (0.254 g, 70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09156827B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-e7d9ea70ca694760a0b4a5e5b630d0fb |
| Source note | uspto-grants-2015_10 |